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Lecturer(s)
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Rejnek Jaroslav, doc. PhDr. CSc.
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Kanický Viktor, prof. RNDr. DrSc.
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Janoš Pavel, prof. Ing. CSc.
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Course content
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1. Overview of spectroscopic techniques for elemental analysis. 2. Principle of optical emission/absorption spectra, principle of mass atomic spectra. 3. Atomic absoption spectrometry: instrumentation, radiation sources, atomizers, monochromatization and detection of radiation, background correction, non-spectral and spectral interferences, elimination or correction of interferences, calibration, examples of analytical methods. 4. Inductively coupled plasma optical emission spectrometry: principle, sample introduction techniques, monochromatization and detection of radiation, types of spectrometers, signal measurement, background correction, spectral and non-spectral interferences, elimination or correction of interferences, measurement optimization and diagnostics, calibration, examples of analytiacl methods. 5. Inductively coupled plasma mass spectrometry: principle, types of mass spectrometers used with inductively coupled plasma ionization source, spectral and non-spectral interferences, elimination or correction of interferences, calibration, measurement optimization, examples of analytical methods, application of ICP-MS as detector for speciation analysis.
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Learning activities and teaching methods
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unspecified
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Recommended literature
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1. Komárek J. Atomová absorpční spektrometrie, Brno, Masarykova univerzita, 2000, ISBN 80-210-2500-X.
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1.Welz B., Sperling. Atomabsorptionsspektrometrie, Weinheim, Wiley - VCH, 1997.
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2. Dočekal B. a kol. Atomová absorpční spektrometrie, Český Těšín, 2 Theta, 1997..
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2.Montaser A., Golightly D. W. Inductively coupled plasmas in analytical atomic spectrometry, Hoboken, N. J., Wiley - VCH, 1992, ISBN 0-471-18811-5.
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3.Nelms S. M. Inductively coupled plasma mass spectrometry handbook, Oxford, Blackwell Publishing, 2005, ISBN 1-4051-0916-5.
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3.Otruba V. (Ed.) a kol. 4. kurz ICP spektrometrie, Brno, Spektroskopická společnost Jana Marka Marci, 2009, ISBN 80-903732-4-0.
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4.Otruba V. (Ed.) a kol. 5. kurz ICP spektrometrie, Brno, Spektroskopická společnost Jana Marka Marci, 2009, ISBN 978-80-903732-8-0.
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