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Lecturer(s)
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Škvorová Magda, Ing. Ph.D.
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Jirsák Jan, doc. RNDr. Ph.D.
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Petrusová Zuzana, Ing. Ph.D.
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Course content
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1. An overview of experimental methods and their division 2. Experimental methods for determination of properties of liquids 3. Experimental method for determination of properties of solids 4. Spectroscopic methods 5. Microscopic methods 6. Electrochemical methods 7. Chromatographic methods 8. Other experimental methods for material characterization 9. Methods available on Department of chemistry for determination of properties of liquids (density, excess molar volumes, refractive index, dissociation constants, chemical composition - AAS, LC, ..) 10. Methods available on Department of chemistry for determination of properties of solids (melting temperature, chemical composition, solid surface characterization - electrokinetic potential, goniometry, AFM, XPS, FTIR, ?) 11. Calculation and estimation methods, overview and division 12. Individual estimation methods for physico-chemical properties determination 13. Electronic formats for description of chemical structures used for estimation methods (SMILES, INChI)
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Learning activities and teaching methods
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unspecified
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Learning outcomes
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This course is focused on presentation of methods for determination of data on physico-chemical properties of pure compounds and mixtures. In the first part of the course, the experimental methods will be presented: their overview, division and usage. Estimation methods for physico-chemical properties will be discussed in the second part of the course.
Students obtain an overview and information about methods for determination of physico-chemical properties of chemical substances. First, the experimental methods for characterization of pure substanes or mixtures in liquid or solid states will be discussed. Then non-experimental approaches will be presented.
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Prerequisites
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There is no preceding course wanted. Students are expected to read and understand the presented texts and to discuss relevant topics during lectures and examination.
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Assessment methods and criteria
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unspecified
Students are expected to read and understand the presented texts and to discussed relevant topics during lectures and examination.
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Recommended literature
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Baum, E. J. Chemical Property Estimation: Theory and Application. CRC Press LLC, USA, 1989.
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POLING, B. E.; PRAUSNITZ, J. M.; O´CONNELL, J. P. The Properties of Gases and Liquids, fifth edition. McGraw-Hill, New York, 2001.
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Slepička, P.; Siegel, J.; Kolská, Z.; Hnatowicz, V.; Švorčík. . Different microscopy approach for solid surface characterization, In: Microscopy: Science, Technology, Applications and Education vol. 2, Formatex Research Center, Badajoz, Spain, pp. 1483-1494 (2010)..
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Zábranský, M.; Kolská, Z.; Růžička, V.; Malijevský, A. Chapter 19. : The estimation of heat capacities of pure liquids. In: HEAT CAPACITIES: liquids, solutions and vapours. Eds. T.M. Letcher and E. Wilhelm. 2010, The Royal Society of Chemistry: London..
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